Lithium-ion batteries have become indispensable in our daily lives, powering everything from our smartphones and laptops to electric vehicles and renewable energy storage systems. To ensure their reliability and longevity, it is crucial to understand the inner workings of these batteries. One of the most advanced techniques for this purpose is Focused Ion Beam Secondary Ion Mass Spectrometry (FIB-SIMS), which provides intricate insights into the composition and behavior of lithium-ion batteries. In this blog, we will explore how FIB-SIMS unravels the secrets of these energy storage wonders.

The Basics of FIB-SIMS

Before delving into how FIB-SIMS characterizes lithium-ion batteries, let’s grasp the fundamentals of this advanced analytical technique. FIB-SIMS combines two powerful methods: Focused Ion Beam (FIB) and Secondary Ion Mass Spectrometry (SIMS). FIB is used to create a precise cross-section of the battery sample, while SIMS is employed to analyze the secondary ions produced when the sample is bombarded with ions.

  1. Sample Preparation

The first step involves preparing a thin cross-section of the battery cell using the FIB, which acts like a microscopic scalpel. This allows researchers to access the internal structure of the battery without damaging its components.

  1. FIB-SIMS Analysis

With the sample ready, the FIB-SIMS instrument comes into play. It uses a focused ion beam to sputter the battery’s surface, releasing secondary ions. These secondary ions are then analyzed using mass spectrometry, revealing the chemical composition of the materials within the battery.

Understanding Lithium-Ion Batteries with FIB-SIMS

Now, let’s explore how FIB-SIMS helps us characterize lithium-ion batteries:

  1. Elemental Composition

FIB-SIMS provides invaluable data about the elemental composition of various battery components. This includes detecting lithium, cobalt, nickel, manganese, and other elements used in the battery’s chemistry. Understanding the exact composition is crucial for optimizing battery performance and safety.

  1. Depth Profiling

FIB-SIMS allows researchers to perform depth profiling. This means analyzing the chemical composition at different depths within the battery. This depth information is essential for monitoring how the materials change over time, particularly as the battery undergoes charge and discharge cycles.

  1. Chemical Mapping

The technique enables the creation of chemical maps for battery components. These maps visually display the distribution of elements and compounds, helping researchers identify regions with potential issues, such as lithium plating, electrode degradation, or uneven distribution of active materials.

  1. Isotope Analysis

FIB-SIMS also has the capability to analyze isotopic compositions. This can provide insights into the source and history of the materials used in the battery, which is vital for quality control and tracing the origin of battery components.

  1. Understanding Degradation Mechanisms

Characterizing a battery with FIB-SIMS is essential for gaining insights into how the materials degrade over time and with repeated cycling. This understanding is fundamental for assessing battery performance and predicting its lifespan.


Focused Ion Beam Secondary Ion Mass Spectrometry (FIB-SIMS) is a cutting-edge technique that allows researchers to dissect the inner workings of lithium-ion batteries with unparalleled precision. By revealing the elemental composition, depth profiles, and chemical changes within these batteries, FIB-SIMS empowers scientists and engineers to enhance battery performance, extend lifespan, and contribute to the advancement of sustainable energy storage solutions. As we continue to rely on lithium-ion batteries for a greener and electrified future, FIB-SIMS plays a pivotal role in unlocking their full potential.

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